Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2,2'-Bis(bromomethyl)-1,1'-binaphthyl | HCID 4185815 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10983494 | HCID 10983494 | — |
Reaction Steps
A mixture of 11.0 g (25 mmol) of 2,2'-bis(bromomethyl)-1,1'-binaphthyl, 4.8 g (51.2 mmol) of phenol, 5.0 g (89.3 mmol) of pulverized potassium hydroxide and 1.14 g (5 mmol) of triethylbenzylammonium chloride is admixed with 30 ml of dichloromethane and stirred for 5 hours at 40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05874642 |
|---|
| Source dataset | uspto-grants-1999_02 |
|---|
| ORD ID | ord-a5d06fbb9888401cb62f79193d29d3da |
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| Source note | uspto-grants-1999_02 |
|---|
