3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one → HCID 13579675, compound

HRID 364088Notes

Reaction equation

HRID 364088 reaction equation
[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14]Cl)[CH2:10][CH2:11][C:5]=2[CH:4]=1.[CH3:21][N:22]([CH3:33])[C:23]1[CH:28]=[CH:27][C:26]([NH:29][CH2:30][CH2:31][NH2:32])=[CH:25][CH:24]=1>>[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][NH:32][CH2:31][CH2:30][NH:29][C:26]3[CH:27]=[CH:28][C:23]([N:22]([CH3:33])[CH3:21])=[CH:24][CH:25]=3)[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 130925103-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-oneHCID 20240086HCID 20240086, compound

Product 1

HCID 13579675HCID 13579675, compound

Procedure

The title compound is prepared from 3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-1-chloropropane and 2-(4-dimethylaminophenylamino)-ethylamine analogously to Example 1.

Sources & evidence

ORD record
ord-7473ce82e0a94f83b6ab8343632c0db1
Source dataset
uspto-grants-1986_08
Patent number
US04604389

Reaction notes

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