HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 5-(3,4-Dimethoxybenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 370314 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
Reaction Steps
After weighing 14.6 g (0.05 mol) of 5-(3,4-dimethoxyphenylmethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (m.p.: 173° C.) to 50 ml of the mixture of formic acid and triethylamine prepared according to Example 1, the procedure described in Example 1 was followed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05414108 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-6e6c0d15e22f49729264b41a77e38132 |
| Source note | uspto-grants-1995_05 |