HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one → N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[3-(4-amino-3,5-dibromo-phenyloxy)-propyl]-methylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one | HCID 13092510 | — |
| Reactant | N-[3-(4-amino-3,5-dibromophenyloxy)-propyl]-methylamine | HCID 20240087 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-[3-(4-amino-3,5-dibromo-phenyloxy)-propyl]-methylamine | HCID 20240073 | — |
Reaction Steps
The title compound is prepared from [3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-1-chloropropane, N-[3-(4-amino-3,5-dibromo-phenyloxy)-propyl]-methylamine and triethylamine analogously to Example 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604389 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-dc4c76c399e2415c9d0fc1287aaa8df3 |
| Source note | uspto-grants-1986_08 |