Butanethiol → HCID 20240462, compound

HRID 364146Notes

Reaction equation

HRID 364146 reaction equation
[OH:1][CH2:2][CH2:3][O:4][C:5](=[O:9])[C:6]([CH3:8])=[CH2:7].[CH2:10]([SH:14])[CH2:11][CH2:12][CH3:13].[OH-].[K+]>>[CH2:10]([S:14][CH2:7][CH:6]([CH3:8])[C:5]([O:4][CH2:3][CH2:2][OH:1])=[O:9])[CH2:11][CH2:12][CH3:13]

Participants

4

Reactant 3

HCID 8012ButanethiolHCID 133602-Hydroxyethyl MethacrylateHCID 14797Potassium Hydroxide

Product 1

HCID 20240462HCID 20240462, compound

Procedure

To the reactor described in Example I was charged 55 grams of 2-hydroxyethylmethacrylate, 37 grams of n-butanethiol, 1.5 grams of Triton™ B and 3 pellets of KOH. The flask contents were reacted at 40° to 50° C. until the reaction was complete by gas chromatography analysis. The yield was theoretical.

Workup

  1. customThe flask contents were reacted at 40° to 50° C. until the reaction

Sources & evidence

ORD record
ord-fe72daee450d4d1cb6a27cd108487f89
Source dataset
uspto-grants-1986_08
Patent number
US04604417

Reaction notes

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