HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 364152Generated: October 30, 2026
Hexamethylenediamine → HCID 67740910, compound
https://huagongshe.com/reaction/364152
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | HCID 53956536 | HCID 53956536 | — |
| Product | HCID 67740910 | HCID 67740910 | — |
Reaction Steps
300 g of allylmethylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride are taken and heated to 130° C., and 79.9 g of melted hexamethylene diamine are added dropwise, with stirring. Water is removed by distillation, the temperature is raised to 180° C. and the pressure is reduced to 53 Pa. 180° C. and 53 Pa are maintained for 15 minutes. This gives 345 g (97% of theory) of a brown, viscous resin having a viscosity of 1.356 Pa.s at 80° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04604437 |
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| Source dataset | uspto-grants-1986_08 |
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| ORD ID | ord-57f95205742e47b6b0325573bd6e0ab4 |
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| Source note | uspto-grants-1986_08 |
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