HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Allyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | tert-Butyl methacrylate | HCID 11448 | — |
| Reactant | HCID 178435178 | HCID 178435178 | — |
| Solvent | Water | HCID 962 | — |
| Product | Allyl methacrylate | HCID 7274 | — |
Reaction Steps
The dimer of allyl methacrylate, which was prepared according to Example 1, was added to the mixture containing 97 wt.-% N-vinylpyrrolidone and 3 wt.-% tert-butyl methacrylate in the amount of 1 wt. % on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 90 wt.-% water at G=0.038 MPa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604440 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-fa4cadfbf86f465b86bc3bbc95423f31 |
| Source note | uspto-grants-1986_08 |