HCID 13689037, compound → HCID 13689033, compound

HRID 364184Notes

Reaction equation

HRID 364184 reaction equation
N[C:2]1C=CC2N(CCN)N=C3C4C=CC=CC=4S[C:3]=1C=23.[NH2:21][C:22]1[CH:30]=[CH:29][C:28]2[N:27]([CH2:31][CH2:32][NH:33][C:34](=O)[CH3:35])[N:26]=[C:25]3[C:37]4[CH:43]=[CH:42][CH:41]=[CH:40][C:38]=4[S:39][C:23]=1[C:24]=23>>[NH2:21][C:22]1[CH:30]=[CH:29][C:28]2[N:27]([CH2:31][CH2:32][N:33]([CH2:2][CH3:3])[CH2:34][CH3:35])[N:26]=[C:25]3[C:37]4[CH:43]=[CH:42][CH:41]=[CH:40][C:38]=4[S:39][C:23]=1[C:24]=23

Participants

3

Reactant 2

HCID 13689037HCID 13689037, compoundHCID 13689038HCID 13689038, compound

Product 1

HCID 13689033HCID 13689033, compound

Procedure

5-amino-2H[1]benzothiopyrano[4,3,2-cd]indazole-2-ethanamine, mp 131°-140° C., hydrochloride salt, mp greater than 300° C. N-[2-(5-amino-2H[1]benzothiopyrano[4,3,2-cd]indazol-2-yl)ethyl]acetamide, mp 213°-216° C., hydrochloride salt, mp 287° C. dec.

Sources & evidence

ORD record
ord-8b55aee5f2e3422d8a19cc587cbae5bb
Source dataset
uspto-grants-1986_08
Patent number
US04604390

Reaction notes

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