HRID364201

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2774217

Ethanamine, 2-bromo-, hydrobromide (1:1)

C2H7Br2N

结构：CCN(CC)CCn1nc2c3c(c(N)ccc31)Sc1cc(OC)ccc1-2

HCID14406786

未命名化合物

PRODUCTS

生成物

结构：Br.CCN(CC)CCn1nc2c3c(c(NCCN)ccc31)Sc1cc(OC)ccc1-2

HCID131714813

未命名化合物

收率 39.9%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Reaction of a solution of 4.5 g (0.0122 mol) of 5-amino-N,N-diethyl-8-methoxy-2H[1]benzothiopyrano-[4,3,2-cd]indazole-2-ethanamine and 7.5 g (0.0366 mol) of 2-bromoethylamine, hydrobromide, in 40 ml of EtOH as described in Example 38 gave 2.4 g of product.