HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 13726314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-Benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one | HCID 13726292 | — |
| Product | HCID 13726314 | HCID 13726314 | — |
Reaction Steps
Following the procedure of Example 1, 4-benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one and dimethylamine were reacted and the free base of the title compound was obtained in the concentrated residue. Recrystallization from ethanol-water gave the product, m.p. 75°-77° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604388 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-bf3c023c58e74a9d9acbd6460d7acffe |
| Source note | uspto-grants-1986_08 |