HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → Ethyl 4-chloro-2-[(cyclohexyloxy)imino]-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate | HCID 54351806 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 4-chloro-2-[(cyclohexyloxy)imino]-3-oxobutanoate | HCID 53775948 | 58.9% |
Reaction Steps
Ethyl 2-cyclohexyloxyimino-3-oxobutyrate (syn isomer, 41.3 g.), acetic acid (41.3 ml.) and sulfuryl chloride (23.8 g.) were treated in a similar manner to that of Example F-(2) to give ethyl 4-chloro-2-cyclohexyloxyimino-3-oxobutyrate (syn isomer, 27.8 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04604456 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-ed8bcea78e484ab594bc9be28a6737a2 |
| Source note | uspto-grants-1986_08 |