HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178454908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178472284 | HCID 178472284 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 178454908 | HCID 178454908 | — |
Reaction Steps
Following the procedure of Example 8, but using 1.96 g of ethyl diethoxymethylphosphinate and 12.5 ml of a 1.6 molar solution of n-butyl lithium in n-hexane and adding 20 ml of 0.1M hydrochloric acid prior to extraction, n-butyl(diethoxymethyl)phosphine oxide is obtained as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05414133 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-974f5591d91b493b9625633d5d34e594 |
| Source note | uspto-grants-1995_05 |