Dipropylamine → HCID 20239561, compound

Participants

Reaction Steps

19.2 g. of 3-chloro-4'-(3-bromopropoxy)-α-ethyl-benzhydrol and 51 ml. of dipropyl amine are refluxed for 8 hours, and the reaction mixture is then evaporated in vacuo. To the residue water is added and it is extracted with benzene. The benzene phase is washed with water, dried over anhydrous magnesium sulfate, and the solution is evaporated under reduced pressure. Distillation of the residue in vacuo yields 11.5 g. of the title compound, boiling at 203° to 206° C./13.3 Pa.

Provenance & Evidence