HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 364668Generated: October 30, 2026
Decalin → 2-Allyl-3-phenyl-7-nitro-1-naphthol
https://huagongshe.com/reaction/364668
Participants
| Role | Name | HCID | Charge |
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| Reactant | Decalin | HCID 7044 | — |
| Reactant | 1-Allyloxy-3-phenyl-7-nitronaphthalene | HCID 20239659 | — |
| Product | 2-Allyl-3-phenyl-7-nitro-1-naphthol | HCID 20239658 | — |
Reaction Steps
31 g of 1-Allyloxy-3-phenyl-7-nitro-naphthalene prepared in step (3) were gradually heated to 180° C. in 390 ml of decaline, the solution being stirred and maintained under nitrogen. The temperature of 180° C. was maintained for about 1 hour. After cooling, the crystals formed were washed with petroleum ether, filtered off and dried at 80° C. under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04605697 |
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| Source dataset | uspto-grants-1986_08 |
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| ORD ID | ord-ce45c7b70cad47a9ad9e28aa5d677ac0 |
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| Source note | uspto-grants-1986_08 |
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