HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → 3-Ethyl-1-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | 3-Ethylphenol | HCID 12101 | — |
| Product | 3-Ethyl-1-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalene | HCID 19095193 | 66% |
Reaction Steps
Employing procedures and materials similar to those described in Example 1, except that 3-ethylphenol was substituted for m-cresol, and the reaction was carried out in the presence of ethylene dichloride as solvent, there was obtained the desired product, 3-ethyl-1-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalene 66% theor., GLC purity 99%+, exhibiting the expected spectral data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04605778 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-b3a280ef250a44ee8ab17496f4e37be6 |
| Source note | uspto-grants-1986_08 |