反应详情

Benzyl (2,6-diisopropylphenyl) ether 60 mg was dissolved in 20 ml of anhydrous ethanol solution of 5% acetic acid. After adding 30 mg of active carbon in 10% palladium thereinto, it was dissolved under hydrogen gas for 15 hours. Thus-obtained mixture Was washed with water and saturated sodium chloride aqueous solution. The resultant was dried with anhydrous magnesium sulfate and then concentrated.

1. dissolutionit was dissolved under hydrogen gas for 15 hours
2. customThus-obtained mixture
3. washWas washed with water and saturated sodium chloride aqueous solution
4. dry with materialThe resultant was dried with anhydrous magnesium sulfate
5. concentrationconcentrated