Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → Benzoyl chloride, 4-(hexyloxy)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4-(Hexyloxy)benzoic acid | HCID 70834 | — |
| 생성물 | Benzoyl chloride, 4-(hexyloxy)- | HCID 170235 | 98% |
반응 단계
Thionyl chloride (485 g of 98%, 4.00 mol) was added dropwise to 300 g (1.35 mol) of 4-hexyloxybenzoic acid. The resulting mixture was refluxed under nitrogen for 2 hours. Distillation yielded 318 g (98%) of 4-hexyloxybenzoyl chloride [boiling point 149°-153° C. (7.5 mm)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04606838 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-37bb1f97559e446dbcf78a51799a51db |
| 출처 메모 | uspto-grants-1986_08 |