HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Pinene → (-) Sodium(4S)-p-menth-1-ene-7-sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Pinene | HCID 14896 | — |
| Reactant | Sodium Bisulfite | HCID 23665763 | — |
| Solvent | Water | HCID 962 | — |
| Product | (-) Sodium(4S)-p-menth-1-ene-7-sulfonate | HCID 23696841 | — |
Reaction Steps
In a 1 liter, 3-neck flask, 70 grams (0.51 mole) β-pinene and 325 ml water was heated to reflux. Sodium bisulfite, 70 grams, was added at the rate of 13 grams per hour. The solution was refluxed for 7 hours and allowed to stand overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04606851 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-535105d41c2445fc90e9acb96f5d350a |
| Source note | uspto-grants-1986_08 |