HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 4-(1,1-Dimethylethyl)-2-dimethylaminomethyleneaminosulfonylanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 5-(Tert-butyl)-2-methoxybenzenesulfonamide | HCID 10933694 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(1,1-Dimethylethyl)-2-dimethylaminomethyleneaminosulfonylanisole | HCID 54498328 | — |
Reaction Steps
4.68 g (0.02 mole) of 3-(1,1-dimethylethyl)-6-methoxybenzenesulfonamide are dissolved in 50 ml of dimethylformamide, and 2.5 g (0.022 mole) of dimethylformamide dimethylacetal are added. The mixture is left to stand for 30 minutes at room temperature and is poured into ice water and the product is filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04607030 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-c16d2080a66843218669fe2072e8e030 |
| Source note | uspto-grants-1986_08 |