HCID 70040791, compound → HCID 70455662, compound

HRID 364931Notes

Reaction equation

HRID 364931 reaction equation
[ClH:1].[NH:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH2:7][C:8]1[CH:18]=[CH:17][C:11]([CH:12]=[CH:13][C:14]([OH:16])=[O:15])=[CH:10][CH:9]=1>O>[OH2:15].[ClH:1].[NH:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH2:7][C:8]1[CH:18]=[CH:17][C:11]([CH:12]=[CH:13][C:14]([OH:16])=[O:15])=[CH:10][CH:9]=1

Participants

3

Reactant 1

HCID 70040791HCID 70040791, compound

Product 1

HCID 70455662HCID 70455662, compoundYield 112.4%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In 35 ml of water, 10 g of 4-(1-imidazolylmethyl)cinnamic acid hydrochloride was dissolved by heating and the solution was allowed to stand overnight at room temperature. The resulting precipitates were collected by filtration and dried at room temperature under reduced pressure to obtain 6 g of 4-(1-imidazolylmethyl)cinnamic acid hydrochloride monohydrate.

Workup

  1. temperatureby heating
  2. customThe resulting precipitates
  3. filtrationwere collected by filtration
  4. customdried at room temperature under reduced pressure

Sources & evidence

ORD record
ord-6c48b09dfb974a3b92fc328a2512029c
Source dataset
uspto-grants-1986_08
Patent number
US04607046

Reaction notes

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