HCID 20238752, compound → 4-(3-Nitrophenoxy)phenol

HRID 364978Notes

Reaction equation

HRID 364978 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[O:7][C:8]1[CH:13]=[CH:12][C:11]([O:14]C)=[CH:10][CH:9]=1)([O-:3])=[O:2].Br.C(O)(=O)C>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[O:7][C:8]1[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 20238752HCID 20238752, compoundHCID 21893785Acetic Acid Mixture with Hydrobromic Acid

Product 1

HCID 132661534-(3-Nitrophenoxy)phenol

Procedure

m-nitrophenol and 4-bromoanisole yield p-(m-nitrophenoxy)anisole of m.p. 69°-71° C. and reaction with hydrobromic acid/acetic acid yields p-(m-nitrophenoxy)phenol which distils in the bulb-tube at 95°-97° C./0.04 Torr;

Sources & evidence

ORD record
ord-8dd752862fc349a09e0e3ebecc283dd3
Source dataset
uspto-grants-1986_08
Patent number
US04607051

Reaction notes

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