HCID 13753170, compound → HCID 13753171, compound

HRID 364979Notes

Reaction equation

HRID 364979 reaction equation
C[O:2][C:3]1[CH:4]=[CH:5][C:6]([O:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[C:7]([CH3:9])[CH:8]=1.Br.C(O)(=O)C>>[O:10]([C:6]1[C:7]([CH3:9])=[CH:8][C:3]([OH:2])=[CH:4][CH:5]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 13753170HCID 13753170, compoundHCID 21893785Acetic Acid Mixture with Hydrobromic Acid

Product 1

HCID 13753171HCID 13753171, compound

Procedure

4-methoxy-o-cresol and bromobenzene yield 5-methoxy-2-phenoxytoluene of b.p. 102°-104° C./0.035 Torr and m.p. 39°-42° C. and reaction with hydrobromic acid/acetic acid yields p-phenoxy-m-cresol; m.p. 96°-99° C.;

Sources & evidence

ORD record
ord-fb95687690674d6a95943be123b69e80
Source dataset
uspto-grants-1986_08
Patent number
US04607051

Reaction notes

Loading…