HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → Ethyl 2-Propyl-3-hydroxy-3-phenylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Ethyl valerate | HCID 10882 | — |
| Product | Ethyl 2-Propyl-3-hydroxy-3-phenylpropionate | HCID 13594173 | — |
Reaction Steps
A 100 milligram sample of the prepared hydroxy-ester is pyrolyzed in a sealed tube at 240°-245° C. for 1 hour. Examination of the pyrolyzate by liquid chromatography indicates that it consists of 60% of unreacted hydroxy-ester and 40% of a 1:1 mixture of ethyl valerate and benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04607118 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-8b090244aaec4db29cb694953bdf1778 |
| Source note | uspto-grants-1986_08 |