HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 13689404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine | HCID 13689358 | — |
| Reactant | 1-Chloro-3-(2-chloroethyl)benzene | HCID 14361215 | — |
| Solvent | Butyl Acetate | HCID 31272 | — |
| Product | HCID 13689404 | HCID 13689404 | — |
Reaction Steps
A mixture of 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (6.05 g, 0.023 mole), 3-chlorophenethyl chloride (4.74 g, 0.027 mole), K2CO3 (10.9 g) and KI (0.1 g) in 130 ml n-butyl acetate was refluxed for 50 hours. The reaction mixture was cooled, filtered and concentrated to an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04608374 |
| Source dataset | uspto-grants-1986_08 |
| ORD ID | ord-a3557218d69a4da580da9976fe127b92 |
| Source note | uspto-grants-1986_08 |