2-[(2,5-Dichlorophenoxy)methyl]oxirane → 1-(2,5-Dichlorophenoxy)-3-[2-(2,6-dimethylphenylamino)-ethylamino]-propan-2-ol

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Reaction Steps

This compound is obtained, in a manner analogous to that described in Example 17, from 2,5-dichlorophenyl glycidyl ether and N-(2,6-dimethylphenyl)-ethylenediamine, the base obtained crystallizing. The desired product is obtained in a yield of 4.2 g. (55% of theory) in the form of colorless crystals which, after recrystallization from diethyl ether-ligroin, melt at 66°-68° C.

Provenance & Evidence