HRID365231

反应详情

EQUATION

反应方程式

HRID 365231 的结构方程式

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

To 288 g of HMDI was added 20 g of cyclohexylamine and they were stirred at 100° C. for one hour while nitrogen was bubbled thereinto and subsequently 2.9 g of the carbodiimidization catalyst was added thereto, after which the resulting mixture was subjected to a reaction at 185° C. for 30 hours, to obtain a carbodiimide resulting from HMDI and having terminal urea bonds (degree of polymerization=10).

WORKUP

后处理

  1. customwas bubbled
  2. additionsubsequently 2.9 g of the carbodiimidization catalyst was added
  3. customafter which the resulting mixture was subjected to a reaction at 185° C. for 30 hours