HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → 3-(n-butylamino)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(n-butylamino)phenol | HCID 11126626 | 57% |
Reaction Steps
0.11 mol of n-butyl bromide and 0.1 mol NaHCO3 are added to 0.1 mol of m-aminophenol in 150 ml of methanol, and the mixture is refluxed for 5 h. After cooling, it is filtered and the solvent is removed in vacuo. The oil which remains is fractionated in vacuo, to give 3-(n-butylamino)phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06126867 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-1d3d42166217481ba4169187abe09eeb |
| Source note | uspto-grants-2000_10 |