HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → Benzenesulfonamide, N-(2-methylpropyl)-3-nitro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Product | Benzenesulfonamide, N-(2-methylpropyl)-3-nitro- | HCID 4591438 | 78.8% |
Reaction Steps
The procedure described in Example 1A was performed using isobutylamine (0.396 g, 5.41 mmol) and 3-nitrobenzenesulfonyl chloride (1.0 g, 4.5 mmol) to give N-isobutyl-3-nitrobenzenesulfonamide (0.916 g, 78%). 1H NMR consistent with structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127372 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-b692aad7b6db4e5591888863b72429b4 |
| Source note | uspto-grants-2000_10 |