HCID 53701357, compound → HCID 54433498, compound

Participants

Reaction Steps

40.0 g of (+/-)-cis-2-ethoxy-1-methoxy-4-(2-nitrocyclohex-4-enyl)benzene are dissolved in 1000 ml of ethanol and 500 ml of tetrahydrofuran, treated with 10 g of Raney nickel and hydrogenated at RT in an autoclave for 4 days at a hydrogen pressure of 100 bar. After filtration and removal of the solvent in vacuo, 35.9 g (99.8% of theory) of the title compound are obtained as a solidifying oil.

Provenance & Evidence