HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 70273938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 23291157 | HCID 23291157 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70273938 | HCID 70273938 | — |
Reaction Steps
1-(t-Butoxycarbonyl)-3-methoxycarbonyl-5-[N-(1-(4-cyanobenzyl)-1H-imidazol-5-yl)acetylamino]piperidine (44.6 mg, 0.093 mmol) was dissolved in CH2Cl2 (6 mL). Trifluoroacetic acid (3 mL) was added and the solution was stirred at ambient temperature for 4 h. The solution was concentrated under reduced pressure to give the title compound without futher purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127366 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-705fc619ad3f46fb8b626853fa4d5f23 |
| Source note | uspto-grants-2000_10 |