4-Methoxybenzenethiol → alpha-[2-(4-Methoxyphenylthio)5-furyl]-N-n-propylnitrone

HRID 365549노트

반응식

HRID 365549 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([SH:9])=[CH:5][CH:4]=1.[CH2:10]([NH:13][OH:14])[CH2:11][CH3:12]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9][C:3]2[O:2][C:11]([CH:10]=[N+:13]([CH2:5][CH2:6][CH3:7])[O-:14])=[CH:12][CH:4]=2)=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 127654-MethoxybenzenethiolHCID 10148984N-propylhydroxylamine

생성물 1

HCID 73433665alpha-[2-(4-Methoxyphenylthio)5-furyl]-N-n-propylnitrone

실험 절차

The title compound was prepared according to the procedure described in Example 1 using 4-methoxybenzenethiol and N-n-propylhydroxylamine. The title compound was isolated in 76.6% yield as slightly yellowish crystals, m.p. 63.0° C. (Rf =0.17 on a silica gel plate using hexanes/EtOAc, 2:1, v:v, as the eluant).

후처리

  1. customThe title compound was prepared

출처 및 근거

ORD 기록
ord-a935aa212a2641dcafa7a1ac80dc1c61
출처 데이터셋
uspto-grants-2000_10
특허 번호
US06127408

반응 노트

불러오는 중…