HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → (2,6-Dimethyl-3-nitrophenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | (2,6-Dimethyl-3-nitrophenyl)methyl acetate | HCID 10537042 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (2,6-Dimethyl-3-nitrophenyl)methanol | HCID 10487641 | 82.4% |
Reaction Steps
To a solution of 2,6-dimethyl-3-nitrobenzyl acetate (26.9 g) in methanol (266 ml) was added aqueous 1N sodium hydroxide solution (133 ml) at ambient temperature for 30 minutes. To the mixture was added water, and the precipitate was collected by filtration to give 2,6-dimethyl-3-nitrobenzyl alcohol (18.0 g) as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127389 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-f1fb1725b3bb469d9f57f73a62124038 |
| Source note | uspto-grants-2000_10 |