化工社化工社 化学情報印刷レポート · 研究参考用
Bromoacetyl chloride → 4-Bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromoacetyl chloride | HCID 89602 | — |
| 反応物 | 2,3,4,5-Tetrahydrobenzo[f][1,4]thiazepine | HCID 12269106 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 4-Bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291657 | 42.1% |
反応手順
2,3,4,5-Tetrahydro-1,4-benzothiazepine (4.8 g), triethylamine (5.9 g) and bromoacetyl chloride (5.5 g) were reacted in the same manner as in Experimental Example 1 to give 4-bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine (3.5 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05416066 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-b064d53212ac4e57835ad8c2d0a85198 |
| 出典メモ | uspto-grants-1995_05 |