HuagongsheHuagongshe Chemistry Print Report · For research reference only
Geraniol → 4-Acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Geraniol | HCID 637566 | — |
| Reactant | 4-Acryloyl-2-chloro-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291658 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | 4-Acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291652 | 68.3% |
Reaction Steps
The above-mentioned 4-acryloyl-2-chloro-2,3,4,5-tetrahydro-1,4-benzothiazepine (1.0 g), geraniol (0.9 g) and zinc chloride (0.8 g) were reacted in the same manner as in Experimental Example 9 to give 4-acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (1.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05416066 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-d9b3e31b5faf42ceb8283b36db1ef77b |
| Source note | uspto-grants-1995_05 |