HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → methyl 1-(2-chlorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | L-Tryptophan, methyl ester | HCID 77980 | — |
| Product | methyl 1-(2-chlorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate | HCID 541453 | — |
Reaction Steps
The same method but starting from racemic tryptophan methyl ester and 2-chlorobenzaldehyde gave the title compound as white crystals m.p.: 154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127542 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-7a44d432676a486e85928259a153decd |
| Source note | uspto-grants-2000_10 |