Ethyl Methacrylate → Ethyl Methacrylate Ethylene Glycol Dimethacrylate

HRID 366290Notes

Reaction equation

CCCCCCCCCCCCOS([O-])(=O)=O.[Na+].S(OOS([O-])(=O)=O)([O-])(=O)=O.[Na+].[Na+].[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][O:47][C:48](=[O:52])[C:49]([CH3:51])=[CH2:50])(=[O:43])[C:40]([CH3:42])=[CH2:41]>>[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][O:47][C:48](=[O:52])[C:49]([CH3:51])=[CH2:50])(=[O:43])[C:40]([CH3:42])=[CH2:41]

Participants

Reactant 4

HCID 7343Ethyl Methacrylate

HCID 7355Ethylene glycol dimethacrylate

HCID 62655Sodium Persulfate

HCID 3423265Sodium Lauryl Sulfate

Product 1

HCID 88089050Ethyl Methacrylate Ethylene Glycol Dimethacrylate

Procedure

Same as C5 except that monomer emulsion was composed of 5 g of SDS, 1 g of sodium persulfate, 180 g of ethyl methacrylate, and 20 g of ethylene glycol dimethacrylate. Tg was 74° C., average particle size was 33 nm and % solids was 20.4%.

Sources & evidence

ORD record: ord-6933989583ad45da8ed81933041a2b35
Source dataset: uspto-grants-2000_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06130014

Reaction notes

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