Methanesulfonyl chloride → HCID 22853533, compound

HRID 36647Notes

Reaction equation

Cl.[CH2:2]([S:6]([NH:9][C@@H:10]([CH2:15][NH2:16])[C:11]([O:13][CH3:14])=[O:12])(=[O:8])=[O:7])CCC.CS([Cl:21])(=O)=O>>[ClH:21].[CH3:2][S:6]([NH:9][C@@H:10]([CH2:15][NH2:16])[C:11]([O:13][CH3:14])=[O:12])(=[O:8])=[O:7]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 22853531HCID 22853531, compound

Product 1

HCID 22853533HCID 22853533, compound

Procedure

23-7 was prepared as described above for the butylsulfonylamino analog (23-6) using methanesulfonyl chloride at the appropriate stage.

Workup

custom23-7 was prepared

Sources & evidence

ORD record: ord-7c78dd1448434d41963455ea8eb9debe
Source dataset: uspto-grants-1995_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05416099

Reaction notes

Loading…