化工社化工社 化学情報印刷レポート · 研究参考用
tert-Butyl chloroacetate → Tert-butyl 5-(biphenyl-4-ylmethyl)-1,1-dioxo-1,2,5-thiadiazolidine-2-acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl chloroacetate | HCID 66052 | — |
| 反応物 | 5-(Biphenyl-4-ylmethyl)-1,1-dioxo-1,2,5-thiadiazolidine | HCID 22615670 | — |
| 反応物 | [4-(4-Chlorophenyl)piperazine-1-sulfonyl]amine | HCID 22615685 | — |
| 生成物 | Tert-butyl 5-(biphenyl-4-ylmethyl)-1,1-dioxo-1,2,5-thiadiazolidine-2-acetate | HCID 54373566 | — |
反応手順
Proceeding as described in Example 7, Step 2 above, but substituting potassium tert-butoxide and [4-(4-chlorophenyl)piperazine-1-sulfonyl]amine with tert-butyl chloroacetate and 5-(biphenyl-4-ylmethyl)-1,1-dioxo-1,2,5-thiadiazolidine gave tert-butyl 5-(biphenyl-4-ylmethyl)-1,1-dioxo-1,2,5-thiadiazolidine-2-acetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06130220 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-0c591902d8d048ebae7ec495dd62e600 |
| 出典メモ | uspto-grants-2000_10 |