HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 366541Generated: October 27, 2026
2-(1-Cyclohexenyl)ethylamine → 3-[2-(Cyclohexen-1-yl)ethyl]-3-azabicyclo[3.1.0]hexane-2,4-dione
https://huagongshe.com/reaction/366541
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-(1-Cyclohexenyl)ethylamine | HCID 76938 | — |
| Reactant | 3-Oxabicyclo(3.1.0)hexane-2,4-dione | HCID 2734721 | — |
| Product | 3-[2-(Cyclohexen-1-yl)ethyl]-3-azabicyclo[3.1.0]hexane-2,4-dione | HCID 23289987 | — |
Reaction Steps
A mixture of 2-(cyclohexen-1-yl)ethylamine (0.59 g) and 3-oxabicyclo[3.1.0]hexane-2,4-dione (0.5 g) was heated at 180° C. for 3 hours. The resulting mixture was cooled to room temperature to give the title compound as a yellow solid, m.p. 60-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06130241 |
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| Source dataset | uspto-grants-2000_10 |
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| ORD ID | ord-eadb4d5121e74d88882f774216a6179b |
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| Source note | uspto-grants-2000_10 |
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