HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydroxybutanedioic Acid → HCID 13725948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydroxybutanedioic Acid | HCID 875 | — |
| Reactant | D-Tartaric acid | HCID 439655 | — |
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | HCID 13725948 | HCID 13725948 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 13725948 | HCID 13725948 | — |
| Product | HCID 102020809 | HCID 102020809 | — |
Reaction Steps
At present, diacetyl tartaric anhydride (DATA) is prepared by reacting tartaric acid with acetic anhydride. Both L-tartaric acid, D-tartaric acid as well as D,L-tartaric acid are not well soluble in acetic anhydride. However, once L-tartaric acid starts to react, it is solubilized in acetic anhydride very quickly. On the other hand, D-tartaric acid and D,L-tartaric acid are not well solubilized. For this reason, DATA is prepared up till now starting from L-(+)-tartaric acid, and consequently, diacetyl-L-tartaric anhydride (L-DATA) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130257 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-7041cc700199439aa91030912ee7af85 |
| Source note | uspto-grants-2000_10 |