HRID36676

反应详情

EQUATION

反应方程式

HRID 36676 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

11.7 g (54 retool) of 6-benzyl-1-methyl-octahydropyrrolo[3,4-b]pyridine as the dihydrochloride are hydrogenated in 100 ml of methanol over palladium-on-active charcoal in accordance with the working instructions of Example Id. Working up by distillation gives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar).

WORKUP

后处理

  1. distillationWorking up by distillation
  2. customgives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar)