HuagongsheHuagongshe Chemistry Print Report · For research reference only
[1-(tert-Butoxycarbonyl)piperidin-4-yl]acetic acid → HCID 23289857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [1-(tert-Butoxycarbonyl)piperidin-4-yl]acetic acid | HCID 1512539 | — |
| Reactant | 8-Chloro-5,11-dihydro-11-(1-piperazinyl)[1]benzothiepino[4,3-b]pyridine | HCID 15780501 | — |
| Product | HCID 23289857 | HCID 23289857 | 83.5% |
Reaction Steps
The title compound (563 mg) was prepared similarly from 1-(8-chloro-5,11-dihydro-[1]benzothiepino[4,3-b]pyridin-11-yl)-piperazine (400 mg, 1.21 mmol) and 1-(1,1-dimethylethoxycarbonyl)-4-piperidine-acetic acid (589 mg, 2.42 mmol); MS (CI, M+H)=557; HRMS: calc.: 557.2353; found: 557.2351.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130229 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-de519ca0d91e4ee591cefd718bc0364f |
| Source note | uspto-grants-2000_10 |