HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane → N-(2-Methylprop-2-enyl)-N-(2-oxoethyl)-urethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane | HCID 15069986 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(2-Methylprop-2-enyl)-N-(2-oxoethyl)-urethane | HCID 15069992 | — |
Reaction Steps
11.5 g (50 mmol) of N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane and 1.25 g (5 mmol) of pyridinium p-toluenesulphate in 100 ml of acetone and 10 ml of water are heated under reflux for two days. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05416096 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-fe5669ce784443e29808812c8f8571c0 |
| Source note | uspto-grants-1995_05 |