HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dehydrolinalool → Linalool
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dehydrolinalool | HCID 62842 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | Linalool | HCID 6549 | — |
Reaction Steps
In a 300 ml pressure reactor, 10 g of the Ru catalyst as described in the catalyst production example were placed in a catalyst basket insert and 150 g (0.99 mol) of dehydrolinalool were added. The hydrogenation was carried out using pure hydrogen at a constant pressure of 40 bar and a temperature of 80° C. After a reaction time of 4 hours, the reactor was vented. The conversion of dehydrolinalool was 95% and linalool was obtained in a selectivity of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130360 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-6e5a1006c86f40c6a0251bc3a7e52998 |
| Source note | uspto-grants-2000_10 |