HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzonitrile → HCID 23287603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzonitrile | HCID 13396 | — |
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Reactant | 2-Chloronicotinic acid | HCID 76258 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 23287603 | HCID 23287603 | 81.3% |
Reaction Steps
The reaction procedure of Example 6 was followed except that 3.60 g (30.64 mmol) of 2-chloronicotinic acid, 20 ml of thionyl chloride, 2.33 g of ammonium thiocyanate and 3.55 g of 4-cyanoaniline were used. As a result, 6.85 g of 2-(4-cyanoanilino)-4H-pyrido[3,2-e]-1,3-thiazin-4-one was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133258 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-c54df5d5d9144a46a152607188a717d2 |
| Source note | uspto-grants-2000_10 |