Ammonium thiocyanate → HCID 23287669, compound

Participants

Reaction Steps

The reaction procedure of Example 102 was followed except that 362 mg of 2-chloronicotinoyl chloride, 156 mg of ammonium thiocyanate, 300 mg of [4-(methylamino)phenyl]acetonitrile and 7 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and chloroform to obtain 347 mg of [4-[N-methyl-N-(4-oxo-4H-pyrido[3,2-e]-1,3-thiazin-2-yl)amino]phenyl]acetonitrile.

Provenance & Evidence