Ammonium thiocyanate → HCID 15485517, compound

Participants

Reaction Steps

The reaction procedure of Example 102 was followed except that 278 mg of 2-chloronicotinoyl chloride, 120 mg of ammonium thiocyanate, 258 mg of -2-(methylamino)benzo[b]thiophene and 6 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and ethyl acetate to obtain 143 mg of 2-[N-(benzo[b]thiophen-2-yl)-N-methylamino]-4H-pyrido[3,2-e]-1,3-thiazin-4-one.

Provenance & Evidence