HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 23287897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | HCID 178418297 | HCID 178418297 | — |
| Product | HCID 23287897 | HCID 23287897 | 85.9% |
Reaction Steps
Using the procedure of Example 20, 6.2 g (20.1 mmol) of 2-dimethylamino-4-mercapto-pyrimidine-5-carboxylic acid (2-piperidin-1-yl-ethyl)-amide were treated with 5.08 g (20.0 mmol) of iodine to give 5.31 g of the title compound after recrystallization from ethyl acetate, mp 128-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133270 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-9c5cde6487cc42c6be294aa861446d3f |
| Source note | uspto-grants-2000_10 |