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HRID36823

反应详情

EQUATION

反应方程式

HRID 36823 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCOc1ccc(-c2ccccc2-c2ccc(C(=O)O)cc2)cc1
HCID131719004

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCOc1ccc(-c2ccccc2-c2ccc(C(=O)Cl)cc2)cc1
HCID131719003

未命名化合物

PROCEDURE

实验过程

After 1.6 g of 4-n-octyloxyterphenyl-4"-carboxylic acid was heated with an excess amount of thionyl chloride under reflux condition for 6 hours, unreacted thionyl chloride was distilled off to obtain 4-n-octyloxyterphenyl-4"-carboxylic acid chloride.

WORKUP

后处理

  1. temperatureunder reflux condition for 6 hours
  2. distillationunreacted thionyl chloride was distilled off