HCID 19936267, compound → HCID 19936256, compound

HRID 36826Notes

Reaction equation

HRID 36826 reaction equation
[CH3:1][CH:2]1[CH2:16][N:15]([CH2:17][C:18]([OH:20])=[O:19])[CH2:14][CH2:13][N:12]([CH2:21][C:22]([OH:24])=[O:23])[CH2:11][CH2:10][N:9]([CH2:25][C:26]([OH:28])=[O:27])[CH2:8][CH2:7][N:6]([CH2:29][C:30]([OH:32])=[O:31])[CH2:5][CH2:4][NH:3]1>C(O)(=O)C>[CH3:1][CH:2]1[CH2:16][N:15]([CH2:17][C:18]([OH:20])=[O:19])[CH2:14][CH2:13][N:12]([CH2:21][C:22]([OH:24])=[O:23])[CH2:11][CH2:10][N:9]([CH2:25][C:26]([OH:28])=[O:27])[CH2:8][CH2:7][N:6]([CH2:29][C:30]([OH:32])=[O:31])[CH2:5][CH2:4][N:3]1[CH2:17][C:18]([OH:20])=[O:19]

Participants

3

Reactant 1

HCID 19936267HCID 19936267, compound

Product 1

HCID 19936256HCID 19936256, compoundYield 49.3%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent2×

Procedure

9 g of crude product 12a are obtained on evaporation of the 0.1M acetic acid. 2.5 g of crude product 12b are obtained on evaporation of the 0.8M acetic acid.

Sources & evidence

ORD record
ord-e126439c08e0494c9b8cac305a3c63b0
Source dataset
uspto-grants-1995_05
Patent number
US05417960

Reaction notes

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